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Textile Research Journal
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An Exploratory Characterization of Cotton Cellulose Modified with Tris (2-chloroethyl)phosphoramide

E.J. Roberts

Southern Regional Research Laboratory,1 New Orleans, Louisiana 70114, U. S. A.

M.A.F. Brannan

Southern Regional Research Laboratory,1 New Orleans, Louisiana 70114, U. S. A.

S.P. Rowland

Southern Regional Research Laboratory,1 New Orleans, Louisiana 70114, U. S. A.

Tris(2-chloroethyl)phosphoramide prepared from ethylenimine and phosphorus oxychloride was reacted with cotton cellulose in the form of print cloth by a pad-dry-cure process involving a base such as sodium carbonate. Relatively low levels of reaction were achieved with this reagent (less than 10% add-on). Conditioned wrinkle recovery angles of the fabric and structural features of the cross links and reagent residues in the cotton cellulose modified with tris(2-chloroethyl)phosphoramide are compared with those of cotton cellulose modified with tris(1-aziridinyl)phosphine oxide.

Key Words: Cellulose • cotton print cloth • tris(2-chloroethyl)phosphoramide • reactants. Chemically • modified cellulose. Textile materials. Dioxane • water • sodium carbonate • potassium carbonate • sodium hydroxide • zine fluoroborate • benzyltrimeth ylammonium hydroxide • catalysts. Concentration • temperature • time. Cross-linking • linkage distribution • electrophore grams • phosphorus content • nitrogen content • chlorine content • structure (reagent residues) • gel fraction • distention index • functionality. Reactions (chemical) • hydrolysis • structural analysis • electrophoresis • diazotization • gas-liquid chromatography.

Textile Research Journal, Vol. 40, No. 8, 699-703 (1970)
DOI: 10.1177/004051757004000805
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